Compliance study for EPA 1613B and EPA 1668C - Part I - in-house test
Compliance study for EPA 1613B and EPA 1668C - Part II - external tests
May 2024
Breaking Ground in Dioxin Analysis: DSP-Systems' Training Session with Micro Electron Optics S.R.L. and Amspec
In a groundbreaking collaboration, DSP-Systems recently joined forces with Micro Electron Optics S.R.L. from Romania and Amspec for an exclusive training session focused on Dioxin analysis.
This innovative program, held at the state-of-the-art facilities of Amspec, aimed to equip professionals from Amspec with the knowledge to use advanced techniques like the Miura GO-EHT and the Shimadzu GC-MSMS for the selective, accurate and precise analysis of Dioxins and PCBs in Grains, Oilseeds, and Oils. The training session kicked off with an introduction to the significance of Dioxin analysis in environmental monitoring. Experts from DSP-Systems and Micro Electron Optics S.R.L. provided valuable insights into the latest methodologies and technologies driving this field forward.
Participants had the unique opportunity to engage in hands-on training, gaining practical experience with the cutting-edge purification and detection equipment. Under the guidance of seasoned professionals, attendees delved deep into the nuances of Dioxin analysis, exploring best practices and troubleshooting techniques.
One of the highlights of the session was the live demonstrations showcasing the capabilities of the Miura GO-HT and the GC-MSMS from Shimadzu. Attendees witnessed firsthand how these advanced instruments streamline the analytical process, delivering accurate and reliable results with unparalleled efficiency. Throughout the training, collaboration and knowledge-sharing were key themes. As the session concluded, participants left with a newfound confidence in their abilities to tackle Dioxin analysis challenges head-on. Armed with cutting-edge techniques and expertise gained from the training, they are poised to make significant contributions to environmental monitoring and regulatory compliance efforts.
The success of this collaborative training session underscores the importance of partnership and innovation in driving progress within the scientific community. DSP-Systems, Micro Electron Optics S.R.L., and Amspec remain committed to pushing the boundaries of Dioxin analysis, paving the way for a cleaner and safer future. Stay tuned for future collaborations and training opportunities as we continue our mission to revolutionize Environmental, Food and Feed analysis and make a positive impact on the world around us.
April 2024
On-site demonstrations in North America now possible
January 2024
A Novel SPE Disk for SPE-03 system
July 2023
SPE-03 Gen4 demonstration
July 2022
Automated purification for PCDD/F and all 209 PCBs (EPA1613B and EPA-1668A)
March 2022:
Increased extraction efficiency of dioxins and PCBs in
fishmeal
September 2021:
The start of Dioxin analysis at Laboratorio Agrama with our first
GO-eHT in Spain
With our GO-2eHT purification system, Centrivap heated vacuum evaporator and CILs complete custom standards solutions kit Manuel (head of R&D) is ready to implement the analysis of Dioxins and PCBs in vegetable oil. During our one week training and implementation session we were able to setup a method of analysis including GC-MSMS measurement and data processing. First results for home-made reference material and an oil PT sample were promising with Trueness between 90-110%, Intermediate Precision around 10% and detection limits around 0.16 pg TEQ/g fat for Dioxins and DL-PCBs.
April 2021:
New column sets for all 209 pcb congeners; current developments
Together with Miura Institute of Environmental Science, Alpha Analytical Laboratories in Mansfield, MA, USA and Quality Testing and Inspection (QTI) in Rotterdam, The Netherlands, we are working on further optimalisation of automated purification of samples for the analysis of all 209 PCB congeners. The existing GO-EHT purification methods are capable methods, delivering suitable recoveries for many PCBs such as NO-, MO- and NDL-PCBs. From many customers, mainly laboratories working on environmental samples we have been receiving requests for column sets which were suitable for the purification of all 209 PCB congeners
By modification of the formulation of the alumina column used for concentrating PCBs, recoveries have substantially been improved, particularly for the high chlorinated ones. Recoveries for all PCB congeners -even the most challenging ones such as # 209- are over 60% and well within the requirements of e.g. EPA 1668. A full application note will be available around the summer of 2021.
Food and feed samples as well as environmental samples can now be analysed for dioxins and PCBs according to EPA 1613 and EPA 1668 methods respectively. GO-EHT systems provides ‘green’ automated sample purification, without DCM, for the analysis of
Dioxins only
Dioxins and PCBs
PCBs only (209 PCB)
PBDEs, PCNs
The new column sets with improved alumina are available from July 2021.
Introducing: Vivace TM Duo: The All-in-one SPE Solution
For high throughput processing of small volume samples
Fast, Light & Versatile
Suitable for PFAS
Vivace™ Duo Solid Phase Extraction system is a dedicated workhorse for the efficient handling of large batches of small biological, food and environmental samples. By running two positions simultaneously, the Vivace™ Duo is twice as fast as single-channel systems on the market. It has a user-friendly touch interface that can store up to 100 methods and apply up to 4 different methods for your sample batch.
Automated sample container rinsing is built-in to improve recovery for sticky compounds such as PFAS. The backdraw feature allows analytes to bypass the syringe pump to eliminate contamination.
NEMC2020: Get the latest news on our 'next generation' sample prep for Dioxins and 209 PCBs.
Douglas G. Hayward, Willem Traag; Chemosphere 256 (2020) 127023
PFAS – Extraction, Purification and Automatization
DSP-Systems visit PromoChrom Technologies in Canada, Richmond, BC
PromoChrom Technologies manufactures smart automated SPE systems for a.o. the extraction of PFAS in water, food and soil samples.
As PromoChrom’s European partner, we will help more laboratories simplify their PFAS extractions in water, food and soil samples! SPE-03 systems are availble now for testing your application(s).
SETAC 2019 Exhibition - November 2-7
Toronto, Canada
Our first exhibition in NA was a success. The 'next generation' sample preparation systems for POPs analysis has officially been introduced in North America! An impression of our booth:
Analysis of Dioxins, PCBs and other POPs without methylene chloride; and < 100ml of solvent use
Presentation of GO-HT technology; next generation of automated sample purification
Poster presentation: The latest news about automated PCB 209 analysis
DSP-Systems enters the North American market with GO-HT technology from Japan.
The first GO-HT systems have been sold to commercial and governmental laboratories
During 2018-2019, GO-HT systems have been tested by several North American laboratories. Food and feed samples as well as environmental samples were analysed for dioxins and PCBs according to EPA 1613 and EPA 1668 methods respectively. GO-HT systems provides ‘green’ automated sample purification, without DCM, for the analysis of
Dioxins only
Dioxins and PCBs
PCBs only (209 PCB method in development)
PBDEs, PCNs
From September onwards, on-site demonstrations in North America are available. We can provide a 2-channel system (GO-2HT) with a set of columns and consumables which enables for the assessment of this next generation technology in your lab. Feel free to contact us!
During Dioxin 2019 in Kyoto, in cooperation with Miura Institute of Environmental Technology (Matsuyama, Japan) the annual GO-HT lunch seminar will be organized.
August 27th, 12:00-13:00h – Room C-1.
Topics will include:
Analysis of all 209 PCB according to EPA 1668
One shot GC-HRMS or GC-MS/MS analysis for PCDD/F & PCBs
Lowering LOQ to answer to EFSA’s opinion for lower background levels
New functions of GO-HT systems
New purification column for fatty samples (High capacity column)
Ongoing: Analysis of 209 PCBs using GO-HT sample purification
In close cooperation with Miura, we are working with priority on developing and optimising a purification method for all 209 PCBs. This application is in particular required for laboratories following EPA 1668 method. Experiments show that the GO-HT is suitable to perform according to EPA regulation. Final experiments are in progress for further optimization of the performance.
Ongoing: High capacity column set
Miura is currently in the finalization stage of developing a higher capacity column set for GO-HT with an improved capacity of up to 5 g fat content. This column set is expected to be available from around Autumn, 2019. More information will follow soon.
New column sets available for environmental (low fat) samples
ᴓ18mm column sets properties and benefits:
Environmental samples
Low fat samples (<1g)
Cost effective
Better elution of mono-PCBs
Faster purification
Test these column sets for your application now: Apply here for 10 column sets free of charge!
New column sets available for DXN only analysis
ᴓ18mm column sets properties and benefits:
Purification of dioxins and furans only
Extra cost efficient
Environmental samples
Low fat samples (<1g)
Faster purification
Test these column sets for your application: Apply here for 10 column sets free of charge!
2019:03 Single injection analysis of PCBs and Dioxin in food and feed using GO-HT sample purification:
2018.12: Feasibility study on Polychlorinated Naphthalenes (PCNs) analysis using GO-HT sample purification
In need for Reference Materials for Contaminants in Food, Soil and Sediment?
Now available on our website: Assigned values for Reference Materials for Contaminant analysis!